Gas Chromatography-Mass Spectrometer (GC-MS), BK-GCMS9600A, ESMC, Biobase, China
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GC-MS, BK-GCMS9600A, Biobase, China
Introduction:
The product integrates the functions of instrument tuning, data processing, and data analysis to improve the operational performance of the instrument and make research work more efficient.
Application:
- Food safety: pesticide residues, flavors, fragrances, additives, packaging materials
- Environmental monitoring: air, water quality, soil, solid waste
- Industrial manufacturing: textiles, cosmetics, electrical and electronic products, plastic products, biomedicine
- Petrochemical: refinery, chemical plant
- Public security system: criminal investigation, explosives, drugs, physical evidence identification
Feature:
1.The temperature and pressure control precision of gas chromatography has reached the international first-class level.
2.The wide temperature RF power supply can adapt to various laboratory environments and perform more stably.
3.High-precision all-metal quadrupole, ensuring good resolution,
4.Quadrupole mass analyzer with pre-quadrupole, more resistant to pollution,
Electron multiplier with high- energy dynode, guaranteeing excellent sensitivity.
6.The high-performance turbomolecular pump ensures the high vacuum environment of mass spectrometry.
7.The inert ion source has high ionization efficiency, and the dual filament design provides double the service time.
8.Autosampler, purge and trap, thermal desorption, and headspace sampler can be configured according to the state of the sample.
Wide-temperature RF power supply can better adapt to various laboratory environments and provide better stability.
The high-temperature inert ion source ionizes efficiently, reduces pollution, and is equipped with two long-life filaments, providing double the service time.
High-precision all-metal quadrupole to ensure good mass spectral resolution.
The imported high- performance turbomolecular pump is adopted, with high pumping speed, stable operation and long life, providing an excellent vacuum environment for mass spectrometry.
Reliable analysis results come from technology that strives for perfection
BK-GCMS9600A has been repeatedly tested with 24 injections of OFN samples, and the RSD is only 0.995%.
Parameter:
| Model |
BK-GCMS9600A |
| Standard Configuration |
MS Unit:
1.GCMS9700A single quadrupole mass spectrometer with workstation software* 1
2. Turbo molecular pump 90l/s* 2
3. Vacuum pump 4m3/h* 1
4. Inert EI ion source* 1
GC Unit:
5.A91PLUS gas chromatograph host, pressure control accuracy 0.001psi *1
6. Split/splitless inlet *1
7. GC Starter Kit
8. MS ion source maintenance kit |
| Option |
24-postions liquid autosampler
Column |
| Power Supply |
220V±10%,50Hz |
| Package Size(L*W*H) |
GC: 960*760*700mm
MS: 780*520*650mm
Pump: 600*300*220mm |
| Gross Weight |
GC: 50kg
MS:55Kg
Pump:22kg |
Application Examples
Environmental Detection Application Example
Test for 16 PAHs Samples
Testing Method
- Instrument used for detection: BK-GCMS9600A
- Column: DB- 5MS, 30m X 0.25mm X 0.25 μ m
- Oven: 50°C (2min) 25°C/min 200°C (0min) 8C/min 300°C (5.5min)
- Source temperature: 270°C
- Transfer line temperature: 280°C
- Injection volume: 1.0μL
- Solvent delay: 5min
- Scan mode: SIM mode; Scan mode
SIM mode chromatographic spectrum of polycyclic aromatic hydrocarbons
Test for 57 VOCs in water
Testing Method
- Instrument used for test: BK-GCMS9600A ; CDS7000 PT
- Column: DB-624, 30m X 0.25mm X 1.4μm
- Oven: 35°C (2min) 5°C/min；120°C (0min) 10°C/min；220°C (2min)
- Source temperature: 240°C
- Transfer line temperature: 250°C
- Injection volume: 5.0mL aqueous solution
- Column flow: 1 .0ml /min
- Solvent delay: 2.0min
- Scan mode: SIM mode
SIM mode chromatographic spectrum of 57 VOCs in water
Testing Examples In The Food Industry
Pesticide residue detection
Testing Method
- Instrument used for test: BK-GCMS9600A
- Column: DB-1701, 30m X 0.25mm X 0.25 μm
- Oven: 40°C (1min) 30°C/min；130°C (0min) 5°C /min；250° (0min) 10°C/min 300°C (5min)
- Source temperature: 240°C
- Transfer line temperature: 280°C
- Solvent delay: 2.0min
- Scan mode: SIM mode
Difenoconazole (cis and trans) Mass lon Chromatogram
Fluoroamide Mass lon Chromatogram
Plasticizer Testing
Testing Method
- Instrument used for test: BK-GCMS9600A
- Column: DB-5MS, 30m X 0.25mm X 0.25 μm
- Oven: 80°C (0.5min) 25°C/min 300°C (4.5min)
- Injection volume: 1μL
- Source temperature: 270°C
- Transfer line temperature: 280°C
- Solvent delay: 3min
- Inlet mode: Split inlet, split ratio 20:1
- Scan mode: SIM mode
Plasticizer DBP, BBP, DEHP m/z= =149 MIC
Example Of Drug Detection In Public Security Department
Example of drug detection
Testing Method
- Instrument used for test: BK-GCMS9600A
- Column: DB- 5MS, 30m X 0.25mm X 0.25 μm
- Inlet temperature: 280°C
- Oven: 60°C (0min) 15°C/min 280C (15min)
- Source temperature: 240°C
- Transfer line temperature: 250°C
- Column flow (constant): 1.0mL/min
- Inlet mode: Split inlet, split ratio 20:1
- Solvent delay: 3.0min
- Scan mode: Full scan, SIM
- Scan mass range: 40 – 500amu
Methamphetamine mass ion chromatogram
Methamphetamine spectral library search
Total ion chromatogram and mass spectrum of 3 fentanyl samples (1 ppm)
Methamphetamine spectral library search
The test results show that the gas chromatography-mass spectrometer is used in the detection of drug methamphetamine samples, with accurate results and simple operation method. Meet the inspection and identification requirements of the public security department for methamphetamine drugs.
For the detection of other drug samples, such as the test of fentanyl mixed standard at 1ppm concentration, the mass spectrum peak shape is good, the separation effect is obvious, the result is stable and the reliability is high.
Examples Of Pesticide Sample Detection
Determination of organochlorine pesticide residues in solid waste
Testing Method
- Instrument used for test: BK-GCMS9600A
- Column: DB-17MS, 30m X 0.25mm X 0.25 μm
- Inlet mode: Pulsed splitless mode
- Inlet temperature: 270°C
- Oven: 40°C (1min) 30°C/min;130°C (0min) 5°C/min;225°C (0min) 10°C/min; 280°C (5min)
- Source temperature: 280°C
- Transfer line temperature: 280°C
- Solvent delay: 5.0min
- Scan mode: Full scan mode; SIM mode
Total ion chromatogram of 19 organophosphorus pesticides
1. Dichlorvos
2. Procymidone
3. Dementon-O+S
4. Ethoprophos
5. Thionazin
6. Sulfotep
7. Thimet
8. Diazinon
9. Disulfoton
10. Dimethoate
11. Fenchlorphos
12. Parathion-methyl
13. Merphos
14. Triadimefon
15. Chlorpyrifos
16. Fipronil
17. Piperonyl butoxide
1 8. Thiodan sulfate
19. Bromopropylate
Images are reference only. Actual product may be different.
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